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"name" : "Bluemel, Janet",
"primaryEmail" : "bluemel@tamu.edu",
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"overview" : "Major research interests in my group include (1) immobilized catalysts, (2) the surface chemistry of oxide materials and (3) solid-state NMR spectroscopy.
Immobilized catalysts (1) allow the advantages of heterogeneous catalysts to be combined with those of homogeneous catalysts. In particular, surface-immobilized homogeneous catalysts are easy to recycle, and can be highly active and selective. Furthermore they are amenable to systematic design. We find the most interesting results when heterobimetallic systems, such as the Sonogashira Pd/Cu catalyst for the coupling of aryl halides and terminal alkynes, are involved. Effective immobilization requires a thorough understanding of the surface chemistry of the oxide support materials (2). Therefore, we investigate not only the reactivity of metal complexes and linkers, but also their mobility on the surfaces.
The most powerful analytical tool for investigating amorphous materials is solid-state NMR spectroscopy (3). We optimized this method especially for surface-bound species, enabling us to study reactions on surfaces, or analyze the nature of our anchored linkers and catalysts.
These different research areas provide my students with a strong multidisciplinary background, spanning from synthetic chemistry, through materials sciences and catalysis, to surface analytical methods including solid-state NMR spectroscopy. Our expertise in these fields has led to many industrial contacts and collaborations.",
"hrJobTitle" : "Professor",
"keywords" : [ "4016 Materials Engineering", "3406 Physical Chemistry", "34 Chemical Sciences", "40 Engineering", "7 Affordable And Clean Energy", "Heterobimetallics", "Fulvalene", "Molybdenum", "Tungsten", "Rhodium", "Liquid Phase", "Wilkinson's Catalyst", "Silica Gel", "Indole", "Supported Catalysts", "Adsorption", "Hybrid Materials", "Structure-property Relationships", "Quantum Dots", "Zinc Oxide", "Colloids", "Solid-state NMR", "Silica Support", "Bifunctional Ligands", "Chelating Ligands", "Immobilized Catalysts", "Barbaralanes", "Tricyclo[3.2.2.0(2,4)]nona-6,8-dienes", "Deprotonation", "1,5-homodienyl Shift", "Bicyclo[3.2.2]nona-2,6,8-trienes", "Paramagnetic Nmr", "Mocvd", "Dative Amine Aluminum Bonds", "Organo-nickel And Iron Complexes", "[2-(n,n-dimethylamino)ethyl]cyclopentadienyl Ligand (cp-n)", "PAEK Polymers", "PEKK-PBI Blends", "PEKK", "High-performance Thermoplastics", "PBI", "Solid-state NMR", "Spectroscopy, Nuclear Magnetic Resonance", "Complex Compounds", "Surfaces", "Interfaces", "Catalysis", "0302 Inorganic Chemistry", "0306 Physical Chemistry (incl. Structural)", "Silanols", "Phosphine Oxides", "Chloroform", "Phenols", "Hydrogen Bonding", "Rietveld Refinement", "Powder Diffraction", "Phosphine", "Silane", "Molecular Rotor", "Rotational Barrier", "Dynamic Nmr", "Macrocycle", "Alkene/olefin Metathesis", "Solid-state NMR", "Hydrogenation", "Platinum", "Biodefense", "Vaccine Related", "Prevention", "3406 Physical Chemistry", "34 Chemical Sciences", "Di(hydroperoxy)alkanes", "Diphosphine Dioxides", "Adducts", "Oxidizing Agents", "Phosphine Oxides", "Peroxides", "Hydrogen Bonding", "Hydrogen Peroxide", "Nuclear Magnetic Resonance (nmr)", "Crystal Structure", "Defects", "Phosphane Ligands", "Solid-state Structures", "NMR Spectroscopy", "Nickel", "Homogeneous Catalysis", "3406 Physical Chemistry", "34 Chemical Sciences", "Silicon Dioxide", "Solvents", "Ions", "Models, Chemical", "Magnetic Resonance Spectroscopy", "Organometallic Compounds", "Pd Catalyst", "Chelating Phosphines", "Linkers", "Ethoxysilanes", "Solid-state NMR", "Immobilization", "Alkene Reduction", "Catalytic Hydrogenation", "P Ligands", "Silica", "Solid-state NMR", "Immobilization", "Rhodium", "0306 Physical Chemistry (incl. Structural)", "Alkyl Chains", "Chelating Phosphines", "Linkers", "Ethoxysilanes", "Solid-state NMR", "Immobilization", "Adsorbed Ferrocene", "H-1 Mas Nmr", "C-13 Mas Nmr", "Chemical Shift Anisotropy", "Adsorbed Chromocene", "Silica Support", "3402 Inorganic Chemistry", "34 Chemical Sciences", "Butadiynes", "Substituent Effects", "Arene Complexes", "Thermolysis", "Chromium Compounds", "3402 Inorganic Chemistry", "34 Chemical Sciences", "3402 Inorganic Chemistry", "34 Chemical Sciences", "Fast Spinning", "Immobilized Catalysts", "P-31 Nmr", "Immobilized Phosphines", "Hh Matching Profiles", "Cp/mas", "Rhodium And Nickel Catalysts", "Silica Supports", "NMR", "Solenoid Probehead", "Carbonylnickel Phosphine Complexes", "Ni-61 Nmr", "NMR", "3402 Inorganic Chemistry", "34 Chemical Sciences", "Union Carbide Catalyst", "Chromocenes", "Solid-state Nmr Spectroscopy", "Metallocenes", "Chromium", "Blends", "Oil And Gas", "Degradation", "Spectroscopy", "Wilkinson's Catalyst", "Olefin Hydrogenation", "Zirconium Phosphate", "Rhodium Nanoparticles", "Immobilized Catalysts", "Hrmas Nmr", "Phosphine Linkers", "Rhodium Catalysts", "Ethoxysilanes", "Olefin Hydrogenation", "Immobilized Catalysts", "Phosphanes", "Isomerization", "Metathesis", "Hydrogenation", "Structure Elucidation", "P Ligands", "Oxidizing Agents", "Phosphine Oxides", "Structure Elucidation", "Hydrogen Peroxide", "Hrmas Nmr", "Phosphine Linkers", "Ethoxysilanes", "Solid-state NMR", "Silica Support", "Immobilized Catalysts", "Stibinosiloxanes", "Antimonites(iii), Silyl-, Oxo-", "Heterosiloxanes", "Nmr, Solid-state", "Cpmas", "NMR", "TiN", "Phosphines", "Oxides", "Surface Properties", "Silicon", "Reference Standards", "Magnetic Resonance Spectroscopy", "Organometallic Compounds", "Binding Sites", "Phillips Catalysts", "Nmr-spectroscopy", "Reversible Oxygen Absorption", "Surface Compounds", "Organochromium Complexes", "Cyclopentadienyl Complexes", "Magnetic Measurements", "Crystal Structure", "Cyclotrimerization", "Nickel Catalysts", "P Ligands", "Silica", "Solid-state NMR", "Immobilization", "Alkynes", "Alkynes", "Silicon Dioxide", "Copper", "Palladium", "Molecular Structure", "Sensitivity And Specificity", "Catalysis", "Magnetic Resonance Spectroscopy", "Organometallic Compounds", "Adsorbed Phosphine Oxides", "Solid-state Nmr Spectroscopy", "Surface Chemistry", "Silica", "Cyclotrimerization", "Nickel Catalysts", "Metallocenes", "NMR Spectroscopy", "Adsorption", "Rhodium Complexes", "Rhodium Nanoparticles", "Chelate Phosphines", "Phosphonium Salts", "Immobilization", "Immobilized Catalysts", "31p Solid-state Nmr", "Silica", "Phosphine Oxides", "X-ray Structures", "Adsorption", "0306 Physical Chemistry (incl. Structural)", "H-2 Isotope Effect", "Natural Abundance H-2- Nmr", "Ehmo Calculation", "H-2 Signal Narrowing", "Paramagnetic Nmr", "Organothallium Compound", "Organoindium Compound", "Crystal Structures", "Olefin Hydrogenation", "Rhodium Complexes", "Solid-state NMR", "Silica Support", "Bifunctional Ligands", "Immobilized Catalysts", "P-31 Suspension Nmr Spectra", "Immobilized Bifunctional Phosphines", "Modified Silica", "P-31 Cp/mas Nmr Spectra", "Immobilized Carbonyl-nickel Phosphine Complexes", "3406 Physical Chemistry", "34 Chemical Sciences", "0306 Physical Chemistry (incl. Structural)", "Steam-treatment Of PBI, PEEK, PEKK", "Water And D2O Uptake Polymers", "Solid-state NMR", "3403 Macromolecular And Materials Chemistry", "3402 Inorganic Chemistry", "34 Chemical Sciences", "Hydroformylation", "Molecular Rotors", "Borohydride Complexes", "Substitution Reactions", "Cage Compounds", "Rhodium", "0306 Physical Chemistry (incl. Structural)", "Dihydroxylation", "Supported Catalyst", "Osmium", "Alkenes", "3402 Inorganic Chemistry", "34 Chemical Sciences", "Alkene Reduction", "P-31", "Catalytic Hydrogenation", "P Ligands", "Silica", "Immobilized Catalysts", "Silica Supports", "Rhodium", "Oxidizing Agents", "Phosphine Oxides", "Peroxides", "Alkanes", "X-ray Structures" ],
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"label" : "Di(hydroperoxy)cycloalkanes Stabilized via Hydrogen Bonding by Phosphine Oxides: Safe and Efficient Baeyer-Villiger Oxidants",
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"label" : "(14)N NMR and two-dimensional suspension (1)H and (13)C HRMAS NMR spectroscopy of ionic liquids immobilized on silica.",
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"label" : "Creating Solid Solutions of Metallocenes: Migration of Nickelocene into the Ferrocene Crystal Lattice in the Absence of a Solvent",
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"label" : "Synthesis, structure, electronic properties and thermal behavior of butadiynyl substituted phenylCr(CO)(3)-complexes",
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"label" : "The Palladium Component of an Immobilized Sonogashira Catalyst System: New Insights by Multinuclear HRMAS NMR Spectroscopy",
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"label" : "Dibridgehead diphosphine dioxide cages: Syntheses and unusual structural features",
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"id" : "n120578SE",
"label" : "THE METALATION OF N,N,N',N'-TETRAMETHYLETHYLENEDIAMINE (TMEDA)",
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"label" : "A Nontemplated Route to Macrocyclic Dibridgehead Diphosphorus Compounds: Crystallographic Characterization of a \"Crossed-Chain\" Variant of in/out Stereoisomers.",
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"label" : "H2O2 adducts of phosphine oxides: Safe, solid, stoichiometric, and soluble new oxidizing agents",
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"label" : "Synthesis and properties of trimesitylthallium. A comparison of the trimesitylelement compounds of group 13",
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"label" : "THE INTRIGUING STRUCTURAL CHARACTERISTICS OF THE HETEROSILOXANE MOLECULE NA4[SB2O(OSIME3)8]",
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"label" : "Surface compounds of transition metals. XLI - Preparation and properties of organochromium compounds by reaction of Phillips catalysts with ethylene",
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"label" : "New mechanistic insights regarding Pd/Cu catalysts for the Sonogashira reaction: HRMAS NMR studies of silica-immobilized systems.",
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"publisher" : "American Chemical Society (ACS)",
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"id" : "n120602SE",
"label" : "PHOTOCHEMICAL 1,2 SHIFT OF THE PHOSPHANE LIGANDS IN THE SILANEDIYL COMPLEX [(2-PH2PCH2C6H4)2SI=CR(CO)5]",
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"label" : "Immobilization and chelation of metal complexes with bifunctional phosphine ligands: A solid-state NMR study",
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"publisher" : "Royal Society of Chemistry (RSC)",
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"label" : "ANALOGS OF METALLOCENES WITH SEPARATED ALLYL AND OLEFIN SYSTEMS",
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"id" : "n398151SE",
"label" : "Chelate phosphine linkers with long alkyl chains for immobilizing catalysts on oxide supports",
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"id" : "n644291SE",
"label" : "Molecular Dynamics and Surface Interactions of Nickelocene Adsorbed on Silica: A Paramagnetic Solid-State NMR Study.",
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"publisher" : "American Chemical Society (ACS)",
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"id" : "n120598SE",
"label" : "NMR-SPECTROSCOPY OF PARAMAGNETIC-COMPLEXES .39. NATURAL ABUNDANCE H-2-NMR OF PARAMAGNETIC SANDWICH COMPOUNDS",
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"publisher" : "Wiley",
"venue" : { }
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"id" : "n401405SE",
"label" : "The Ferromagnetic Coupling Mechanism in Hetallocenium/-Anion Stacks as seen by NMR Spectroscopy",
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"publisher" : "Taylor & Francis"
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"id" : "n411442SE",
"label" : "Hydrogen peroxide adducts of triarylphosphine oxides.",
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"publisher" : "Royal Society of Chemistry (RSC)",
"venue" : { }
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